PEMBUATAN CMC (CARBOXY METHYL CELLULOSE) DARI SELULOSA ECENG GONDOK DENGAN MEDIA REAKSI CAMPURAN LARUTAN PROPANOL-BUTANOL

L. BATU, DYVIA ROSA APRILYANTY (2016) PEMBUATAN CMC (CARBOXY METHYL CELLULOSE) DARI SELULOSA ECENG GONDOK DENGAN MEDIA REAKSI CAMPURAN LARUTAN PROPANOL-BUTANOL. Other thesis, POLITEKNIK NEGERI SRIWIJAYA.

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Abstract

Waterhyacinthisoneofaquaticweeds which is able to disturbaquaticecosystemproblem.Manyeffortsweremadetoreduce thenegativeimpact oftheseplants, at oneofthembyusing itas rawmaterialforsynthesisofCarboxymethylCellulose(CMC).WaterHyacinthhashighpotentialtobeCMCbecauseitscellulosecontentisquiteat 60%. The purpose of this research is to make CMC from water hyacinth which is still less utilization as well get optimum conditions of solvent and sodium acetate to the CMC resulted.In this research, making CMC from water hyacinth is done by the process of alkalization and karboksimetilation. The first step cellulose hyacinth mixed with a solvent mixture of propanol-butanol using a variety of solventpropanol-butanol (20:80, 50:50, 80:20) and then alkalization using 10% NaOHsolution.The next step is karboksimetilasi reaction between the alkali cellulose and sodium chloroacetic (ClCH2COONa) with variations ClCH2COONa (9 grams, 12 grams, 15 grams.) The analysis conducted in this study is the degree of substitution, pH, viscosity, NaCl concentration and purity. In this research, it is gotten that the CMC with optimum conditions on the composition of propanol-butanol 20:80 solvent with the degree of substitution of 0.92, pH 7.7, viscosity 9, purity of 96.9% and a weight of 9 grams ClCH2COONa with the highest degree of substitution of 0.76 pH 7.2, 8 viscosity and purity of 96.95%.

Item Type: Thesis (Other)
Uncontrolled Keywords: Eceng gondok, Karboksimetil Selulosa (CMC), Derajat Substitusi
Subjects: T Technology > TP Chemical technology
Divisions: Chemical Engineering > Undergraduate Theses
Depositing User: Mrs Trisni Handayani
Date Deposited: 27 Feb 2017 02:20
Last Modified: 27 Feb 2017 02:20
URI: http://eprints.polsri.ac.id/id/eprint/3313

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